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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-54
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-54
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filingDate 2000-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7f4058e44164104d7c295dfd6b0662c7
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publicationDate 2002-01-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2002003448-A
titleOfInvention Method for producing 2-alkyl-2-adamantyl (meth) acrylate
abstract PROBLEM TO BE SOLVED: To provide an alkyl group obtained by alkylation of adamanthanone and -OH or -OM {M is an alkali metal or M gX (X is a halogen). } Having a 2-alkyl or 2-alkylidene adamantane derivative, Provided is an efficient and highly pure purification method of crude 2-alkyl-2-adamantyl (meth) acrylate reacted with an acrylic acid derivative. SOLUTION: A crude 2-alkyl-2-adamantyl (meth) acrylate is heated at a temperature and for a time of t ≦ exp {(A / T) + B} where A and B are crude 2-alkyl-2-adamantyl (meth) acrylates. Is a constant determined from the relationship between the heating temperature and the time at which the decomposition amount reaches a specific ratio using a standard sample having substantially the same composition. }, And thin-film distillation is performed so as not to cause decomposition of 2-alkyl-2-adamantyl (meth) acrylate.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-4667593-B2
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priorityDate 2000-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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