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filingDate 2000-06-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2001-02-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2001039952-A
titleOfInvention Process for producing N-alkyl-N'-methylalkylene urea substantially free of formic acid
abstract (57) [Summary] (with correction) [PROBLEMS] N-alkyl-N ′ containing substantially no formic acid -To provide a method for producing methyl alkylene urea. [Solution] Expression: [Where R 1 is HCH 3 ; R 2 is C n H 2n + 1 (n = 1 to 4); x represents 0,1]. N-alkyl-N′-methylalkylene urea substantially free of formic acid represented by the formula: is reacted with the corresponding alkylene urea in the presence of formic acid to form monomeric formaldehyde or formaldehyde With N-alkyl-N′- obtained by the reaction. A mixture of methylalkylene urea and formic acid is fed to the upper region of the distillation column and distilled without any addition, and N-alkyl-N'-methylalkylene urea substantially free of formic acid is distilled in the lower region of the distillation column. At that time, the pressure in the upper region of the distillation column was set at a level 10 to 100 mbar higher than that in the lower region, and the temperature in the lower region of the distillation column was set at 4 higher than the upper region. It is characterized in that it is set to a level higher by 0 to 210 ° C.
priorityDate 1999-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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