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filingDate 1996-03-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2000-08-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2000510878-A
titleOfInvention Method for producing polytetramethylene ether glycol diester over aluminum-magnesium silicate catalyst
abstract (57) Abstract: fixed bed - by polymerization of tetrahydrofuran in the presence of a polymerization catalyst and a carboxylic acid anhydride of the formula: R-CO-O (-CH 2 -CH 2 -CH 2 -CH 2 -O) n - An improved process for preparing a polytetramethylene ether glycol diester represented by COR 1 wherein R and R 1 are the same or different and represent an alkyl group or a derivative of an alkyl group. By using neutral or weakly basic magnesium-aluminum-hydrosilicate catalysts in place of the known acidic montmorillonite-, zeolite- or kaolin catalysts, heavy polymerizations with higher polymerization rates, uniform properties and narrow molecular weight distributions are obtained. Coalescence can be obtained even with industrial quality tetrahydrofuran.
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