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filingDate 1997-04-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2000-07-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2000509040-A
titleOfInvention Method for producing aluminoxanes
abstract (57) [Summary]nWater, hydrocarbylaluminum (eg, trimethylaluminum) and organic solvent (eg, toluene) are fed to the reactor under controlled ratios and temperature control to produce a dilute reaction product mixture having the specified composition and concentration. The solution is then mixed with at least two product mixtures, one of which is hydrocarbylaluminum dissolved in an organic solvent essentially free of aluminoxane, and the other is essentially a hydrocarbylaluminum. An organoaluminum compound consisting of hydrocarbylaluminum and hydrocarbylaluminoxane is a concentrated solution in which the amount of aluminoxane is much higher in the organic solvent than the amount of hydrocarbylaluminum]. Water is supplied through an orifice that is surrounded by a stream of solvent to bring the water into the solvent solution containing the hydrocarbyl aluminum compound and / or aluminoxane in the solvent stream, thereby transferring the water to the hydrocarbyl aluminum compound and Advantageously, it is added to the solvent solution containing the aluminoxane.
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