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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C409-16
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-22
filingDate 1997-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2000-07-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2000508332-A
titleOfInvention Process for producing 2,5-dimethyl-2,5-di-tert-butylperoxyhexane
abstract (57) [Summary]nIn order to produce 2,5-dimethyl-2,5-di-t-butylperoxy-hexane, 2,5-dimethyl-1,5-hexadiene and t-butyl hydroperoxide were completely dissolved in an anhydrous solvent under an acidic catalyst. The reaction is carried out in the presence of an electron pair acceptor-Lewis acid therein. If industrial water-containing t-butyl hydroperoxide is used, it is mixed with 2,5-dimethyl-1,5-hexadiene, then the water is removed after addition of sulfuric acid or calcium chloride, followed by electron pairing. An acceptor Lewis acid can be added.
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