http://rdf.ncbi.nlm.nih.gov/pubchem/patent/IN-2014DN05755-A

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filingDate 2012-12-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_87c28d2e13fba6ad7a62660bdfe76386
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publicationDate 2015-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber IN-2014DN05755-A
abstract Methods of isolating a 4 chloro 2 fluoro 3 substituted phenylboronate include adding carbon dioxide gas or carbon dioxide solid (dry ice) to a solution comprising a 4 chloro 2 fluoro 3 substituted phenylboronate an inert organic solvent and at least one lithium salt to react the at least one lithium salt with the carbon dioxide gas or carbon dioxide solid (dry ice) and form a mixture comprising the 4 chloro 2 fluoro 3 substituted phenylboronate the inert organic solvent and a precipitated solid. The precipitated solid may be removed from the mixture. Methods of using 4 chloro 2 fluoro 3 substituted phenylboronates to produce methyl 4 amino 3 chloro 6 (4 chloro 2 fluoro 3 substituted phenyl)pyridine 2 carboxylates are also disclosed. A 4 chloro 2 fluoro 3 substituted phenylboronate produced by one of the methods of isolating a 4 chloro 2 fluoro 3 substituted phenylboronate is also disclosed wherein the 4 chloro 2 fluoro 3 substituted phenylboronate may be obtained at a yield of greater than or equal to about 90%.
priorityDate 2011-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 25.