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filingDate 1976-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 1977-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber IE-44314-L
titleOfInvention IMPROVEMENTS IN THE MANUFACTURE OF 4-CHLORO-2-BUTYNYL-¹n-(3-CHLOROPHENYL) CARBAMATE
abstract In the process for manufacturing 4-chloro-2-butynyl m-chlorocarbanilate (the herbicide barban) from the corresponding 4-hydroxy-2-butynyl m-chlorocarbanilate it has been discovered that yields and product quality are improved by employing dimethylformamide as reaction promoter in combination with thionyl chloride or phosgene as chlorinating agent.n[US4012433A]
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