http://rdf.ncbi.nlm.nih.gov/pubchem/patent/HU-T53110-A

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filingDate 1989-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4c1b3630d3686ee3b8da430848279652
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8067586b989efffb20e267b46f9489c6
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publicationDate 1990-09-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber HU-T53110-A
titleOfInvention Process for neutralizing waste mother lye containing acetic acid and for utilizing the acetic acid content in the form of potassium acetate
abstract To render acetic acid contg. waste mother liquors harmless, acetic acid is reclaimed as potassium-acetate. 1-5 mols. - of ethanol are added for each mol. of acetic acid and 8-10 wt.% of sulphonic acid based on mother-liquor wt.. This mixt. - is distilled at or below 78 deg.C.. Any methyl-acetate collected in the fraction is distilled off. - Ethanol is extracted from the residual base fraction of water so for every 4 mols. ethylacetate, a mixt. of 2-3:8-12:3-5 molar proportion, of water:ethanol:potassiumhydroxide is added and reacted at 50 deg.C. max. 45-66 wt.% of this mixt. is removed by distn. at atmospheric pressure. To the remainder 0.5-2.5 mols. of water are added for each mol. of potassium hydroxide used originally for hydrolysis. This mixt. is distilled off with a distn. temp. of 100 dec.C is obtd. The residue contains potassium-acetate, which is subjected to opt. purifcn. and/or concn..
priorityDate 1989-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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