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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-20
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C57-03
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C57-02
filingDate 1992-12-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_66b0e7c2449302e7c79c1c84d7848724
publicationDate 1997-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber HU-213385-B
titleOfInvention Process for the preparation of ethyl-4-(trichloro-acetamido)-5-hexenoate
abstract The present invention relates to a novel process for the preparation of ethyl 4- (trichloroacetamino) -5-hexenoate. According to the present invention, (i) dehydrated and formylated in the presence of erythritol formic acid during a thermal reaction; (ii) reacting the resulting 4- (formyloxy) -3-hydroxy-1-butene with triethyl orthoacetate under thermal reaction conditions to give ethyl 6- (formyloxy) -4-hexenoate in the presence of ethanol and hydrochloric acid. Converted to 6-hydroxy-4-hexanoate; (iii) converting the thus obtained ethyl 6-hydroxy-4-hexenoate by reaction with trichloroacetonitrile to ethyl 6- (trichloroacetimidyloxy) -4-hexenoate and then rearranging this compound thermally. EN 213 385 B Scope of the description: 5 pages (including 2 sheets)
priorityDate 1991-12-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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