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filingDate 1987-05-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6343dd4e4ff4e37d10a132379e78b73a
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publicationDate 1989-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber HU-198006-B
titleOfInvention Process for working up 4-nitro-acetophenon mother liquours containing dinitro-ethyl-benzene
abstract Potentially explosive, di:nitro-ethyl-benzene contained in a mother liquor of 4-nitro-acetophenone is processed industrially to render it safe, as follows, (i) mother liquor placed in a short dwell time vessel is distilled with, pref. superheated steam. The head-product contg. mainly 4-nitro-ethyl-benzene is returned into the oxidn. process, (ii) the secondary mother liquor (the bottom prod.), which contains mainly 4-nitro-acetophenone found also in a short dwell time vessel, is distilled at a reduced pressure with steam or superheated steam, (iii) 4-nitroacetophenone is extracted from the head product and (iv) opt. operations (i), (ii) and (iii) are repeated and (v) finally any residual matter is destroyed.
priorityDate 1987-05-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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