http://rdf.ncbi.nlm.nih.gov/pubchem/patent/HU-192848-B

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b2bf6236ce5d340612ff62a106d6c013
filingDate 1983-09-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b782101d11500dbcefd58ba05ade29a3
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d81c0eb42523e5ea2721ebf644e0d061
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8db49605712eeb72d585d86ee1960264
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publicationDate 1987-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber HU-192848-B
titleOfInvention Process for preparing azo-dicarboxylic acid diamide
abstract The target cpd. is prepd. by mixing 43-100 pts. by wt. 30-70 wt.% aq. urea soln. under intense stirring with 100 pts. by wt. of an aq. soln. contg. 130-150 g per litre sodium-hypochlorite and 150-170 g per litre sodium-hydroxide. The resulting mixt. is fed through a heating zone to raise its temp. in 0.1-1.0 minutes to 110-130 deg.C and added to an aq. soln. contg. 0.76 mole equivs. inorganic or organic acid for each mole urea. The temp. of the reaction mixt. is kept at 130-150 deg.C and its pH at 7-8 until extracted samples stop consuming iodine. The resulting hydrazo-dicarbonic acid-diamide is oxidized by known methods to the azo cpd. which is sepd. from the suspension, washed and dried. - The process yields the target cpd. which is widely used in the plastics industry in a simple and economic way.
priorityDate 1983-09-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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