http://rdf.ncbi.nlm.nih.gov/pubchem/patent/GB-950543-A

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filingDate 1962-03-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 1964-02-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber GB-950543-A
titleOfInvention Recovery of by-product adipic acid
abstract Adipic acid is recovered from a crude mixture of cyclohexanol and cyclohexanone prepared by the oxidation of cyclohexane in a liquid phase by molecular oxygen, by steam distilling the crude in a stripping zone, removing and cooling the tails from the stripping zone to 20-40 DEG C. and maintaining at that temperature for at least one hour to crystallise the adipic acid which is separated and washed. The cooling stage may be under a pressure of 10 mm. mercury, and the product may be washed with a mixture of cyclohexane, and refined cyclohexanone-cyclohexanol. Specification 806,660 is referred to.
priorityDate 1961-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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