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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D241-44
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D241-44
filingDate 1950-05-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 1953-07-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber GB-694497-A
titleOfInvention Preparation of 2-sulfanilamidoquinoxaline
abstract 2-Sulphanilamidoquinoxaline is prepared by heating a mixture of 2-haloquinoxaline, sulphanilamide and an acid-binding agent, particularly an alkali or alkaline earth carbonate, bicarbonate or hydroxide. The temperature may be between 120 DEG and 180 DEG C. In an example, 2-chloroquinoxaline, sulphanilamide and potassium carbonate are heated together to 160-165 DEG C. for five hours, cooled, diluted with water, acidified to pH9 to separate unchanged sulphanilamide, and then acidified and cooled to 0-5 DEG C. to precipitate the 2-sulphanilamidoquinoxaline.
priorityDate 1949-05-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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