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publicationDate 2015-11-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber GB-2525950-A
titleOfInvention Process
abstract A process for the production of dialkyl succinate from bio-succinic acid comprising: (a) feeding solid bio-succinic acid to a reactor and contacting with alkanol, (b) passing a stream removed from the reactor comprising unreacted succinic acid, mono-alkyl ester, dialkyl ester, alkanol, water and impurities to the top of a reaction zone column, passing said stream in counter-current reaction to upflowing alkanol, (c) removing a stream from the bottom of the reaction-zone column and passing it to a bottoms-stream separation zone where said dialkyl ester is separated from the other components; (d) recycling the succinic acid and mono-alkyl ester to the reaction-zone column; (e) removing the impurities as a purge; and (f) removing a stream from the top of the reaction-zone column and passing said it to a top-stream distillation zone where the alkanol is separated from the other components and recycling the organic components to the reaction-zone column.
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