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filingDate 1975-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 1978-04-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber GB-1508067-A
titleOfInvention Process for preparing indanthrene dyes
abstract 1508067 Process for preparing indanthrene dyes PRODUITS CHIMIQUES UGINE KUHLMANN 20 June 1975 [21 June 1974] 26227/75 Heading C4P Vat dyes of the dianthraquinone-azine or dianthraquinone-N,N<SP>1</SP>-dihydroazine series, or a higher cyclic homologue thereof are prepared by reacting an optionally further substituted primary aminoanthraquinone or a higher cyclic homologue thereof with an alkaline condensing agent in presence of at least one N-oxide of an aliphatic or aromatic amine, N-oxide of a heterocyclic organic nitrogenous base, alkylphosphine oxide, arylphosphine oxide, alkylaminophosphine oxide, alkylarylaminophosphine oxide or arsine oxide. Preferred compounds include hexamethylphosphorotriamide, pyridine-N-oxide, quinoline- or isoquinoline-N-oxides, and dimethyl-aniline-N-oxide. The reaction preferably takes place in presence of an oxidizing agent e.g. air or oxygen, a solvent and a wetting agent at 50‹-140‹C. The preferred reactants are 1-amino-anthraquinone and sodium or potassium hydroxide.
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priorityDate 1974-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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