http://rdf.ncbi.nlm.nih.gov/pubchem/patent/GB-1290922-A
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B47-067 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B67-0026 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B67-50 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B47-067 |
filingDate | 1970-02-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 1972-09-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | GB-1290922-A |
abstract | 1290922 Preparing metal phthalocyanines DAINICHISEIKA COLOR & CHEMICALS MFG CO Ltd 13 Feb 1970 7136/70 Heading C4P Metal phthalocyanines are prepared by condensing an o-dinitrile of the general formula wherein A forms an aryl or a heterocyclic radical, X is H, halogen, nitro, amino, sulphonic or carboxylic acid group, alkyl or alkoxy and n is an integer from 1 to 4, and a metal or a metal compound capable of providing the central metal atom of a phthalocyanine pigment at below 100‹ C. in presence of an alkaline substance which is an hydroxide, oxide, peroxide or carbonate of an alkali metal or alkaline earth metal and a hydrophilic organic solvent containing an hydroxy group. A copper phthalocyanine, produced by the above method and having an X-ray crystallographic pattern with peaks at 6À8, 9À8, 15À6, 24À8, 25À2, 25À6, 26À8 of 2#(CuKα/Ni) is claimed per se. The hydrophilic organic solvents used include C 1 -C 4 alcohols, ethylene glycol, propylene glycol, polyethylene glycol, polypropylene glycol, methyl and ethyl Cellosolve diethylene-glycol ethyl ether, phenol and o-, m- and p-cresols. The o-dicyano compound is preferably of the benzene, naphthalene, anthracene or phenanthrene series and the metals used include Co, Cu, Ni, Zn, Sn, Fe, Pd, Cr, Pt, Mn, V and Mo and their compounds. In preferred embodiments (i) a hydrophobic organic solvent may replace part of the hydrophilic organic solvent, e.g. benzene, toluene, xylene, naphthalene, biphenyl, chlorobenzenes and naphthalenes, nitrobenzene, chloronitrobenzene, and nitrotoluene; and the condensation may take place in presence of (ii) an inorganic or organic ammonium salt, (iii) an acid, (iv) a surfactant, (v) a compound forming a complex with the metal atom. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4077973-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2018053135-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4783386-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2152808-A1 |
priorityDate | 1970-02-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 57.