http://rdf.ncbi.nlm.nih.gov/pubchem/patent/GB-1030259-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b9fa13c33b79ba86e25d61d5e3cee4f2 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C323-59 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C323-58 |
filingDate | 1964-10-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_dfeaaad9b5348c031ca391442e08147c |
publicationDate | 1966-05-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | GB-1030259-A |
titleOfInvention | Improvements in the production of n-acetyl-l-cysteine |
abstract | N-acetyl-L-cysteine, is made by acetylating L-cystine in the presence of barium hydrate solution with ketene or acetic anhydride, to form N.N1 diacetyl-L-cysteine which is treated with sulphuric acid to remove barium as a precipitate of barium sulphate, and is then electrolytically reduced to N-acetyl-L-cysteine. Preferably a diaphragm cell is used with sulphuric acid as anolyte and the acid solution of the acetylated cysteine as catholyte. A carbon anode, and a cathode of tin, lead, mercury, or nickel which may be coated with platinum. Power at 12V, 5 Amps is applied, and the product solution is neutralised, concentrated and crystallized.ALSO:N: N1 - diacetyl-L-cystine is made by acetylating L-cystine in the presence of barium hydrate solution with ketene or acetic an-hydride. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110615749-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/AU-714021-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-6159352-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110615749-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2108654-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-9742358-A1 |
priorityDate | 1964-10-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 45.