http://rdf.ncbi.nlm.nih.gov/pubchem/patent/FR-2769983-A1

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filingDate 1997-10-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fc2365417dea92c4e05978fe9f1a1e8b
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publicationDate 1999-04-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber FR-2769983-A1
titleOfInvention PROCESS FOR HEAT ATTACK IN OXIDIZING CONDITIONS OF A CERAMIC
abstract The invention relates to a method of thermal etching under oxidizing conditions of a ceramic with a view in particular to revealing its grain boundaries and studying its granular microstructure. particular to UO2 and to mixtures (U, Pu) O2. Said thermal attack is carried out in a furnace with a controlled atmosphere constituted by an oxidizing gas providing a chemical potential of oxygen of -75 kJ / mol to -125 kJ / mol, and comprises the following successive stages: - rapid rise in temperature of the furnace at a speed of 900degreC / h to 1500degreC / h from the initial temperature to a temperature plateau; - maintaining the temperature at said plateau at a value of 1250degreC to 1450degreC for a period of 30 minutes to 15 minutes.
priorityDate 1997-10-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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