Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5d664eed04da4901936792151acc51f5 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-3813 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-38 |
filingDate |
1975-06-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0926912b86e0c5beb7c6283818b812af http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4669024d5fd06c06612e754a2a94f8a3 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_dd86473c0987c7868f8c8c3515603d4a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_40f2ee3f564ac7437b7c7ecb0847c07e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b8c094e8d5dd2725bbf762f88299ae0f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_81c5a2a93eed76dd2b4176b82b4438f7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_94250470beedb132d1d8b950b8cf51f4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0161bcfdb0f6db352ae77dd249e445f5 |
publicationDate |
1976-01-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
FR-2276312-A1 |
titleOfInvention |
PROCESS FOR PREPARING N-PHOSPHONO-METHYLENE-GLYCINE AND ITS DISODIUM SALT |
abstract |
N-Phosphonomethyl-glycine (I) and its salts are produced by reacting glycine with chloromethylphosphoric acid (II) or a salt thereof in is not 35% caustic alkali (pref. NaOH) at elevated temp. (pref. 90-105 degrees C), the pH of the reaction mixture being held at >10 by addition of solid alkali hydroxide if necessary, after completion of the reaction separating off the resulting alkali chloride, acidifying the filtrate isolating the resulting (I), and converting (I) into a salt if desired. (I) and its disodium salt are known plant growth regulators and herbicides. Using >35% caustic alkali and maintaining pH >10 by adding solid alkali hydroxide simplifies purification procedures and shortens reaction times without adversely affecting yields. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-7750180-B2 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2005019230-A3 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/FR-2568882-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2005019230-A2 |
priorityDate |
1974-06-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |