http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-320732-A1
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b04b60a0fd911e0e9a8c9dd5c7654a8d |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C209-36 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C201-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-12 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-06 |
| filingDate | 1965-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 1966-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | ES-320732-A1 |
| titleOfInvention | N-DIETHYL AMINO ACETYL 2, 4, 6 TRIMETHYL ANILIDE MANUFACTURING PROCEDURE |
| abstract | "MANUFACTURING PROCEDURE OF N-DIETILE AMINO ACETYL 2,4,6-TRIMETHYL ANILIDE" characterized in that the glacial acetic acid in a flask equipped with a stirrer and thermometer is introduced into a cold bath, gradually adding fuming nitric acid mixing at 10º C to add mesitylene, keeping the temperature at less than 20º C; then adding acetic anhydride maintaining the temperature between 25-30º C and allowing the mixture to cool for two hours at room temperature and then heating at 50º C for ten minutes, then letting it cool; pouring the product on a mixture of ice and salt for the precipitate of the obtained nitrated derivative, filtering it, washing it extracting it with petroleum ether; washing the ethereal extracts with aqueous alkaline solution, drying with calcium chloride, distilling the solvent and recrystallizing the residue in methyl alcohol. (Machine-translation by Google Translate, not legally binding) |
| priorityDate | 1965-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 29.