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publicationNumber ES-2688169-T3
titleOfInvention Procedure for the production of nitroalkanes in a microstructured reactor
abstract Process for the production of nitroalkanes by reacting at least one alkane with at least one nitrating agent in the gas phase, characterized in that the nitration is carried out in a microstructured reaction zone with parallel channels with hydraulic diameters of less than 2.5 mm and a total specific internal surface of more than 1600 m2 / m3, where the alkane and nitrating agent are transported in gaseous form at a pressure of 1 bar to 20 bar through the reaction zone and are transformed at a temperature of 150 ° C to 650 ° C and the reaction products are cooled and evacuated after the reaction zone, and where a mixture of nitrogen oxides and oxygen is used as at least one nitrating agent, where a partial mixture rich in nitrogen oxide is fed to the reactor inlet and an oxygen-rich partial mixture is fed through two to ten feed points throughout the reaction zone.
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