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grantDate 2017-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2017-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2639062-T3
titleOfInvention Process for the preparation of polyamides
abstract Process for the preparation of a polyamide based on dicarboxylic acids and diamines consisting of the steps of: A) Provide a mixture of aqueous monomers of dicarboxylic acids and diamines, wherein the molar ratio of dicarboxylic acids to diamines is adjusted such that at the end of step C) there is a molar deficiency of dicarboxylic acids or diamines of between 1 and 10 mol%, based on the other respective component, B) Transfer the aqueous mixture from step A) to an operating evaporation reactor continuous, in which the diamines and carboxylic acids are reacted at a temperature in the range between 100 and 370 ° C and a pressure in the range between 1 and 50 bar, C) Transfer the mixture from step B) to a separator , which is operated at a temperature in the range between 100 and 370 ° C and at a pressure in the range between 1 and 50 bar, with separation of the gaseous components, D) Transfer the mixture from step C) together with diamine or acid dicarboxy In a suitable quantity to balance the molar excess, to a tubular reactor, which is operated at a temperature in the range between 100 and 370 ° C and at a pressure in the range between 1 and 50 bar, during a residence time in the range between 10 seconds and 30 minutes, E) Transfer the mixture from step D) to an extruder, which is operated at a temperature in the range between 150 and 400 ° C, during a residence time in the range between 10 seconds and 30 minutes, while the gaseous components are separated through degassing holes, wherein the monomer mixture of step A) consists of a mixture of dicarboxylic acids of between 60 and 88% by weight of terephthalic acid and between 12 and 40% by weight of isosphthalic acid, where up to 20% by weight of the carboxylic acid mixture can also be replaced by other dicarboxylic acids, and hexamethylene diamine, of which up to 20% by weight can be replaced by others C2-30-diamines.
priorityDate 2009-12-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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