http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2620578-T3

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filingDate 2013-11-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2017-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f5e4d6184cae02fac57416069152f7a8
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publicationDate 2017-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2620578-T3
titleOfInvention Treatment of a mixture of CDON and CDOL using a column sequence with lateral discharge
abstract A process for the separation of a target fraction (A) rich in cyclododecanone from a mixture of dehydrogenation O containing compounds that boil at low temperature (LB), cyclododecanone (CDON), compounds that boil at medium temperature (MB), cyclododecanol (CDOL) and high temperature boiling compounds (HB) characterized by the following steps: a) make available the dehydrogenation mixture (O); b) distillate the compounds that boil at low temperature (LB) from the dehydrogenation mixture (O) by obtaining a first mixture (ABC1) comprising cyclododecanone (CDON), compounds that boil at medium temperature (MB) , cyclododecanol (CDOL) and high temperature boiling compounds (HB); c) feed the first mixture (ABC1) into a primary column with lateral discharge (7); d) discharge a first fraction (A1) rich in cyclododecanone from the head of the primary column with lateral discharge (7); e) discharge a first fraction (C1) containing cyclododecanol (CDOL) and compounds boiling at high temperature (HB) from the sump of the primary column with lateral discharge (7); f) discharge a second mixture (ABC2) comprising cyclododecanone (CDON), cyclododecanol (CDOL) and compounds that boil at medium temperature (MB) from the lateral outlet of the primary column with lateral discharge (7); g) feed the second mixture (ABC2) into a secondary column with lateral discharge (8); h) discharge a second fraction (A2) rich in cyclododecanone from the head of the secondary column with lateral discharge (8); i) discharge a second fraction (C2) containing cyclododecanol (CDOL) and high temperature boiling compounds (HB) from the sump of the secondary column with lateral discharge (8); j) discharge a third mixture (ABC3) comprising cyclododecanone (CDON), cyclododecanol (CDOL) and compounds that boil at medium temperature (MB) from the side outlet of the secondary column with lateral discharge (8); k) gathering the first fraction (A1) rich in cyclododecanone and the second fraction (A2) rich in cyclododecanone by obtaining the target fraction (A) rich in cyclododecanone.
priorityDate 2012-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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