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publicationDate 2017-02-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2600037-T3
titleOfInvention Procedure for the preparation of 2,2-difluoroethylamine from 2,2-difluoro-1-chloroethane and ammonia
abstract Process for the preparation of 2,2-difluoroethylamine, which comprises the following steps: (I) Mix 2,2-difluoro-1-chloroethane and gaseous, liquid or supercritical ammonia in a pressure-stable and closed reaction vessel, at a pressure in the range of 1000 to 18000 kPa; (II) reacting the reaction mixture at a reaction temperature in the range of 80 ° C to 200 ° C; (III) Allow the reaction mixture to stand and remove 2,2-difluoroethylamine, no solvent being used in the present procedure.
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Total number of triples: 27.