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filingDate 2005-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2012-09-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2386898-T3
titleOfInvention Method for manufacturing difluoromethane
abstract A process for the production of difluoromethane (HFC-32), the process comprising: (a) providing a reaction vessel; (b) providing activated carbon impregnated with a strong Lewis acid fluorination catalyst in which the strong Lewis acid catalyst is selected from the Sb halides in the reaction vessel; (c) activating the catalyst by passing through the activated carbon impregnated with the strong Lewis acid fluorination catalyst, anhydrous hydrogen fluoride gas and chlorine gas; (d) contacting, in a vapor state in the reaction vessel containing the activated catalyst, hydrogen fluoride and dichloromethane at a temperature in the range of 60 ° C to 200 ° C to produce a product stream comprising difluoromethane (HFC-32) and one or more of hydrogen chloride, unreacted chlorinated hydrocarbon reactant (s), low fluorinated intermediates and unreacted hydrogen fluoride and (e ) separate difluoromethane (HFC-32) from the product stream.
priorityDate 2004-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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