http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2379311-T3
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b468caeef13bcea1721145591daefcda |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-10 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D301-12 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D301-12 |
filingDate | 2008-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2012-04-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_23634ead9f69d8f1dae384d95f87251a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6163b079ae52e2e8feda34f036c3695f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_50fd9032cd61645cf6e756101dd60905 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1f00cffe2b8717626bbc90d43e966466 |
publicationDate | 2012-04-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | ES-2379311-T3 |
titleOfInvention | Procedure for the preparation of epichlorohydrin |
abstract | Procedure for the preparation of epichlorohydrin, with quea) being carried out in a first reaction stage, allyl chloride and hydrogen peroxide are reacted in the presence of a zeolite-type catalyst containing titanium in a molar ratio of the allyl chloride to hydrogen peroxide of at least 1: 5: 1, and containing the allyl chloride employed 1-chloropropane and / or 2-chloropropane, b) the reaction mixture formed in the first reaction stage, is separated, in a distillation, in a mixture (A), which contains the unreacted allyl chloride, as well as 1-chloropropane and / or 2-chloropropane, and in a mixture (B), which contains epichlorohydrin, c) the mixture (A) is subdivided into a mixture (A1), which is returned to the first reaction stage, and in a mixture (A2), d) the mixture (A2) is reacted in a second reaction stage with hydrogen peroxide in the presence of a catalyst of the type of zeolite containing titanium in a molar ratio of the allyl chloride to hydrogen peroxide, which is in the range of 0.5: 1 to 1, 25: 1, e) the reaction mixture formed in the second reaction stage is separated, in a distillation, in a mixture (C), which contains 1-chloropropane and / or 2-chloropropane, and in a mixture (D), which contains epichlorohydrin and f) the mixture (C) is removed from the process. |
priorityDate | 2008-03-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 40.