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publicationDate 2011-06-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2360508-T3
titleOfInvention PROCEDURE TO RECOVER CAPROLACTAMA FROM A WATERPROOF CAPROLACTAM PRODUCT USING PREPARED ALCALINE AMINOCAPROATE IN SITU.
abstract Continuous process for recovering caprolactam from an aqueous caprolactam product, said aqueous caprolactam product comprising (i) caprolactam, (ii) impurities and (iii) water, said process comprising: - adding alkali metal hydroxide to the aqueous caprolactam product , in an amount less than 20 mmol of alkali metal hydroxide per kg of caprolactam; and - reacting at least 50 mol% of the alkali metal hydroxide added to form alkaline aminocaproate to obtain a caprolactam product enriched in caproate before a subsequent distillation step; and - distilling the caprolactam product enriched in caproate under reduced pressure.
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