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grantDate 2009-11-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2009-11-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2328250-T3
titleOfInvention ALCOXILATIONS IN MICROSTRUCTURED CAPILLARY REACTORS.
abstract Process for the production of polyether alcohols of the general formula (I) ** see formula ** by alkoxylation of compounds of the general formula R 1 (XH) m in a microstructured reactor with series of channels connected in parallel for conducting chemical reactions between essentially liquid reaction partners, optionally in the presence of a solid catalyst, where the conduction of the chemical process takes place in spaces that are formed by two or more plates or layers of essentially parallel faces, in which the mixing of the reactants takes place individually in a single phase in a liquid state in each reaction channel and a heat exchanger device is provided, namely a cooling or heating device, and the reactor is designed for pressures up to 800 bar and temperatures in the range of - 30 ° C to 400 ° C, characterized in that the compound R 1 (XH) m and an appropriate catalyst is mixed n and introduced into the reactor, fed to the reactor 1 to 300, preferably 2 to 150 equivalents of alkylene oxide directly or at various points and mixed with the compound R 1 (XH) m, catalyst and / or its by-products, they are transformed into the reaction channels at a temperature in the range of 50 to 300 ° C and a pressure in the range of 11 to 800 bar and then the product mixture is cooled, where R 1 in the formula R 1 ( XH) m represents a mono- or polyvalent organic moiety, m represents a corresponding integer, R 2 is the same or different in the molecule and represents hydrogen and / or an organic moiety, particularly CH 3, C 2 H 5, phenyl, C 10 H 21, or allyloxymethyl, X represents O, S, NH or NR '', and R '' is a cyclic or acyclic organic moiety, optionally substituted with 1 to 26 carbon atoms.
priorityDate 2004-03-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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