http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2265441-T3

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filingDate 2001-08-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2007-02-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2d654ddb638840f0f82113f8c244fe3b
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8cd9fefe197243da00f5f08eecdb9573
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publicationDate 2007-02-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2265441-T3
titleOfInvention PROCEDURE FOR THE PREPARATION OF AMMONIUM-STABLE NITRILS AGAINST HYDROLYSIS.
abstract Process for the preparation of stable ammonium nitriles against hydrolysis, by reaction of a compound of Formula 1, Formula 1 in which R1, R2, R3 are the same or different, and represent C1-C24 alkyl groups or C2 alkenyl groups - C24, linear or branched, or C1-C4 alkoxy-C1-C4 alkyl groups, or represent substituted or unsubstituted benzyl, or in which R1 and R2 in common with the nitrogen atom, to which they are attached, form a ring with 4 to 6 C atoms, which may be substituted with C1-C5 alkyl, C1-C5 alkoxy, C1-C5 alkanoyl, phenyl, amino, ammonium, cyano, cyanamino, chlorine or bromine, and which, in addition to the nitrogen atom , instead of carbon atoms, it may contain one or two oxygen or nitrogen atoms, an N-R6 group or an R3-N-R6 group, wherein R6 is hydrogen, C1-C5 alkyl, C2-C5 alkenyl, C2-C5 alkynyl, phenyl, C7-C9 aralkyl, C5-C7 cycloalkyl, C1-C6 alkanoyl, cyanomethyl or cyano, R4 and R5 are hydrogen, C1-C4 alkyl , C1-C4 alkenyl, C1-C4 alkoxy-C1-C4 alkyl, phenyl or C1-C3 alkyl-phenyl, preferably hydrogen, methyl or phenyl, meaning R4 in particular hydrogen, when R5 does not mean hydrogen, and A represents an anion, with a compound of the formulas RSO3X, R1SO4X or R2CO2X, meaning R, R1 and R2 C4-C20 alkyl, preferably C10-C18, or substituted aryl, preferably C1-C18 alkyl-phenyl, and meaning X an alkali metal ion, of ammonium or hydrogen, the nitriles of Formula 1 being dissolved in water at 50 to 100 ° C, until saturation, mixing with an aqueous solution, saturated in the same temperature range, of the compounds of the formulas RSO3X, R1SO4X or R2CO2X , and the sulphonates, sulfates and ammonium nitrile carboxylates being separated, after cooling the mixture.
priorityDate 2000-08-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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