http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2245584-A1

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ca34960070f4ac7a1b77cec4c3f5be0f
filingDate 2004-02-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ed607493ddf68bb94acf705bc98e56d8
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aeaabaab5f8f687f729a8e0afc60c413
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_27ee7ff496b7a4403932b95b2a31d582
publicationDate 2006-01-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber ES-2245584-A1
titleOfInvention PROCEDURE OF ELECTROCHEMICAL HYDROXYLATION FROM MONOCARBOXYL ACIDS OF QUINOLINE OR ITS CARBOXYLATES, TO PRODUCE HYDROXY-QUINOLINES AND QUINOLONES.
abstract Electrochemical hydroxylation procedure anfrom quinoline monocarboxylic acids or their carboxylates,nto produce hydroxy-quinolines and quinolones.n n n Electrochemical hydroxylation procedure anfrom quinoline monocarboxylic acids or their carboxylates,nto produce hydroxy-quinolines and quinolones.n n n The electrochemical synthesis ofnhydroxy-quinolines and quinolones used asnreagent compounds 2-quinolinic acid (I) orn4-quinolinic acid (II), or its correspondingncarboxylates. This synthesis is carried out through a process ofnelectrochemical reduction and gives rise to compounds derived fromnhydroxy-quinolines and quinolonesn3,4-dihydro-2-quinolone andn3-hydroxyquinoline (IV).n n n In the synthesis can be used very diversenmaterials such as cathodes and anodes. The catholyte and anolyte may benseparated, or not, by a selective, non-selective membrane or andiaphragm. The catholyte consists of an aqueous solution or not ofnone of the starting compounds I or II and a suitable electrolyte.nThe anolyte consists of an aqueous solution or not of ansuitable electrolyte. The electrolysis is performed between 0 and 90 ° C, atna pH between 0 and 14, with a current density between 1nmA / cm2 and 2 A / cm2 and / or a cathode potential betweenn(-0.5) V and (-3.0) V vs. Ag / AgCI.
priorityDate 2004-02-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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