http://rdf.ncbi.nlm.nih.gov/pubchem/patent/ES-2234138-T3
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_cd2955c27933428d2aa5701f1ba09d5c |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-188 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-1804 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61Q19-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K8-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K8-58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K8-55 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F7-18 |
filingDate | 1998-08-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2005-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_10465a37f8057ad5849c672153721006 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1a1ea16034af5d17dd658c4f0dec66bc |
publicationDate | 2005-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | ES-2234138-T3 |
titleOfInvention | PREPARATION WITH HIGH PURITY ALCOXITRIMETILSILANOS FLUIDS. |
abstract | Process for the production of a liquid alkoxytrimethylsilane of general formula: RO-SiMe3 wherein Me is methyl and R is a substituent of monovalent aliphatic hydrocarbon having from 14 to 20 carbon atoms, said fluid being substantially free of organic and inorganic compounds, whose process comprises the steps of: (a) melting a solid alcohol of the general formula R-OH wherein R is defined as above; (b) catalyzing said molten alcohol with 20 to 200 ppm of trifluoromethanesulfonic acid; (c) reacting said catalyzed molten alcohol at a temperature ranging from 10 ° C above the melting point of said alcohol to 100 ° C in an anhydrous inert atmosphere, with at least a stoichiometric equivalent amount of a trimethylsilylation agent; (d) separating any reaction byproduct and excess trimethylsilylation agent; (e) neutralize the trifluoromethanesulfonic acid catalyst with an excess of an anhydrous base; and (f) separating salts, from said liquid alkoxytrimethylsilane, by filtration. |
priorityDate | 1997-10-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 60.