http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-3921301-A1

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filingDate 2020-02-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e4498c6ba95a18f2b436e86cc96ea286
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publicationDate 2021-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-3921301-A1
titleOfInvention Process for producing 4,4'-dichlorodiphenyl sulfoxide
abstract The invention relates to a process for producing 4,4'-dichlorodiphenyl sulfoxide comprising: (a) reacting thionyl chloride, chlorobenzene and aluminum chloride in a molar ratio of thionyl chloride : chlorobenzene : aluminum chloride of 1 : (6 to 9) : (1 to 1.5) at a temperature in the range from 0 to below 20°C, forming an intermediate reaction product and hydrogen chloride, (b) mixing aqueous hydrochloric acid and the intermediate reaction product at a temperature in the range from 70 to 110°C to obtain a crude reaction product comprising 4,4'-dichlorodiphenyl sulfoxide, (c) separating the crude reaction product into an organic phase comprising the 4,4'-dichlorodiphenyl sulfoxide and an aqueous phase, (d) washing the organic phase with an extraction liquid.
priorityDate 2019-02-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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