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filingDate 2016-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_951b5a1cd754bef111a575a5706c91a3
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publicationDate 2019-05-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-3480185-A1
titleOfInvention Method for preparing polythiol compound, method for preparing curable composition, and method for producing cured product
abstract Provided is a method for producing a polythiol compound, the method including: step 1 of reacting 2-mercaptoethanol having a water content of 3000 ppm or less on a mass basis, with epihalohydrin to obtain a halide represented by the formula (1), wherein X represents a halogen atom; step 2 of reacting the halide represented by the formula (1) with an alkali metal compound selected from the group consisting of an alkali metal sulfide and an alkali metal hydroxide to obtain a polyol compound selected from the group consisting of a polyol compound represented by the formula (2) and a polyol compound represented by the formula (3); step 3 of reacting the polyol compound with thiourea in the presence of an acid to obtain an isothiuronium salt; step 4 of hydrolyzing the isothiuronium salt in the presence of a base to obtain a polythiol salt; and step 5 of converting the polythiol salt into a polythiol by an acid to obtain at least one polythiol compound selected from the group consisting of a polythiol compound represented by the formula (4), a polythiol compound represented by the formula (5), a polythiol compound represented by the formula (6), and a polythiol compound represented by the formula (7).
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