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publicationDate 2018-10-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-3389812-A1
titleOfInvention Recovery column for the purification of acrylonitrile/acetonitrile mixtures
abstract A process for separating acrylonitrile from a mixture of acrylonitrile and acetonitrile includes providing a mixture of acrylonitrile and acetonitrile to a recovery column; contacting the mixture of acrylonitrile and acetonitrile with aqueous solvent to provide an acrylonitrile-water azeotrope; and separating the acrylonitrile-water azeotrope from the acetonitrile to provide an overhead stream that includes the acrylonitrile-water azeotrope and about 0.05 weight percent or less acetonitrile, a bottoms stream that includes about 0 to about 0.0075 weight percent acetonitrile, and a sidestream that includes about 5 to about 70 weight % acetonitrile.
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