http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-2748139-A1

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filingDate 2012-10-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4ae77d499fb8a9d1969a59a61cdfd5e3
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publicationDate 2014-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-2748139-A1
titleOfInvention Process for the hydrodechlorination of a liquid feed comprising dichloroacetic acid
abstract The process of the present invention pertains to a process wherein a liquid feed comprising monochloroacetic acid, dichloroacetic acid,and optionally acetic acid and/or trichloroacetic acid is subjected to a catalytic hydrodechlorination step by contacting it with a source of hydrogen in the presence of a solid heterogeneous hydrogenation catalyst situated in a fixed catalyst bed, wherein the liquid feed is fed to the top of avertical tubular reactor at a superficial mass velocity of between and 10 kg/s per square meter of the horizontal cross-section of the vertical tubular reactor and a rate of between 250 and 3,000 kg/hr per m of said catalyst bed, wherein the source of hydrogen is fed to the top or bottom of the vertical tubular reactor at a rate of between 0.025 to 0.25 Nm/s per square meter of the horizontal cross-section of the vertical tubular reactor, so as to obtain an average axial pressure gradient of at least 2 kPa per meter of said catalyst bed, and wherein the temperature in the top of the vertical tubular reactor is between 100 and 200°C, and wherein the pressure in the top of the vertical tubular reactor is between 0.2and 1.0 MPa.
priorityDate 2011-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 30.