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filingDate 2010-07-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2012-05-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-2456733-A2
titleOfInvention Methods of forming sintered boron carbide
abstract A method of forming a sintered boron carbide body includes washing boron carbide powder with essentially pure water at an elevated temperature to generate low oxygen boron carbide powder, mixing a sintering aid and a pressing aid with the low oxygen boron carbide powder to form a green mixture, and shaping the green mixture into a green boron carbide body. The method can include mixing titanium carbide powder having an average particle diameter in a range of between about 5 nm and about 100 nm with the low oxygen boron carbide powder. The method can further include sintering the green boron carbide body, and hot isostatic pressing the sintered body, to a density greater than about 98.5% of the theoretical density (TD) of boron carbide. Alternatively, the method can include sintering the shaped boron carbide green body at a temperature greater than about 2,200 0C, to thereby form a eutectic liquid solid solution of B4C/SiC, forming a sintered boron carbide body with a density greater than about 98% TD.
priorityDate 2009-07-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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