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publicationDate 2011-01-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-2270237-A2
titleOfInvention Method for manufacturing arabinoxylan
abstract Process for the preparation of water-soluble arabinoxylan from common wheat flour by means of the process steps Preparation of a flour-water suspension, maintenance of a resting time of the flour-water suspension of 3-10 minutes, dilution of the flour-water suspension with circulating water, decanting of the flour-water suspension Suspension by means of a three-phase decanter in a centrifugal field, separation of the obtained upper run in a further centrifugal field, recycling the heavy fraction obtained in the further centrifugal field in the starch recovery cycle, addition of α-amylase to light fraction obtained in the further centrifugal field, dextrinating the light fraction with a jet cooker, storage of the hydrolyzate with flocculation and sedimentation in a reaction vessel over 0.3 to 13 hours and a pH of 1 to 10, centrifuging the sediment, grinding drying of the sediment, saccharification of the clarified and dextrinated hydrolyzate in a stirred reactor medium s glucoamylase with simultaneous proteolysis with a mixture of an alkaline and a neutral protease, ultrafiltration of the hydrolyzate via a multi-stage ultrafiltration, whereby a permeate and a retentate are obtained and the amount of retentate is only one fifth of the starting amount. Evaporation of the permeate until a concentration of 50 to 90% dry matter is reached, evaporation of the retentate until a concentration of 20 to 50% dry matter is reached, recycling the two evaporator vapor condensates in the starch process, precipitation of the evaporated retentate up to an ethanol concentration of 60 to 80% by mass in a semi-batch mode operation formed by a stirred reactor containing 94 to 99% by volume of ethanol at a temperature of 5 to 70 ° C, further comprising a high speed rotor-stator mixer, an addition possibility of concentrated retentate into a bypass inlet of the rotor-stator mixer under vacuum conditions, filtering and washing the filter cake with 94 to 99% by volume ethanol at least once, followed by mill-drying of the water-soluble dietary fiber concentrate prepared in the manner described, and workup and R recycling of the ethanol used for washing, as well as the produced feed and uses for the produced glucose concentrate.
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