http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1984335-B1
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_9b449501522aa74c4e7883dcee4f8200 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-46 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-44 |
filingDate | 2007-02-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2009-08-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_07ce1e0b4b80e35dff71e8ee4eba9db6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d03d386058a3d44e511461b95057a82e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1e7cdd009c25aa3f29c5e2a0edf09880 |
publicationDate | 2009-08-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | EP-1984335-B1 |
titleOfInvention | Improved process for the preparation of stable nitroxyl radicals |
abstract | Process for the preparation of stable nitroxyl radicals (I) starting from N-benzylphthalimide in two steps. In the first step, the intermediate N-benzyl-1, 1, 3, 3-tetra- alkylisoindoline is prepared by treatment with a Grignard reagent, prepared in methyl-tert-butyl ether, of N- benzylphthalimide, obtained in the same reaction environ - ment starting from phthalic anhydride and benzylamine. In the second step, the N-benzyl-1, 1, 3 , 3-tetra- alkylisoindoline is transformed into the nitroxyl radical by hydrogenolysis and subsequent oxidation with hydrogen peroxide in the presence of a catalyst selected from acids and salts of polymolybdic or polytungstic acids. |
priorityDate | 2006-02-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 64.