http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1723154-A2

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/H01L21-265
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B6-10
filingDate 2005-01-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ef360391fdc056ef6d4182401e394642
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ad61dda28be790973359bc437270eeac
publicationDate 2006-11-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-1723154-A2
titleOfInvention Isotopically-enriched boranes and methods of preparing them
abstract The invention provides new methods for synthesis of large boron hydride clusters, e.g., boron hydride molecules of the formula BnHm where 5≤n≤96 and m≤n+8, wherein m and n satisfy the electron counting rules of macropolyhedral boranes. The invention is particularly useful for synthesis of octadecaborane (B18H22). Preferred methods of the invention include iteratively generating a conjugate acid from a salt of the [BaHb]c- or [Bn+2Hm-4]2- anion followed by degradation under conditions conducive to concentrating and drying of the conjugate acid to provide a borane BnHm and residual salt of the [BaHb]c- or [Bn+2Hm-4]2- anion which is reused in the method of synthesis. The invention further provides isotopically enriched boranes, particularly isotopically enriched 10B18H22 and 11B18 H22.
priorityDate 2004-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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