http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1723154-A2
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ac39f2b350f9ca20552b16c240220b8b |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-582 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B6-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01L21-2658 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B6-10 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/H01L21-265 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B6-10 |
filingDate | 2005-01-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ef360391fdc056ef6d4182401e394642 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ad61dda28be790973359bc437270eeac |
publicationDate | 2006-11-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | EP-1723154-A2 |
titleOfInvention | Isotopically-enriched boranes and methods of preparing them |
abstract | The invention provides new methods for synthesis of large boron hydride clusters, e.g., boron hydride molecules of the formula BnHm where 5≤n≤96 and m≤n+8, wherein m and n satisfy the electron counting rules of macropolyhedral boranes. The invention is particularly useful for synthesis of octadecaborane (B18H22). Preferred methods of the invention include iteratively generating a conjugate acid from a salt of the [BaHb]c- or [Bn+2Hm-4]2- anion followed by degradation under conditions conducive to concentrating and drying of the conjugate acid to provide a borane BnHm and residual salt of the [BaHb]c- or [Bn+2Hm-4]2- anion which is reused in the method of synthesis. The invention further provides isotopically enriched boranes, particularly isotopically enriched 10B18H22 and 11B18 H22. |
priorityDate | 2004-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 51.