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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C209-48
filingDate 2004-09-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4339a91ddb1a19c26b9773e0b343761b
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publicationDate 2006-06-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-1663946-A1
titleOfInvention Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile
abstract The invention relates to a method for the production of diaminoxylene, by continuous hydrogenation of liquid phthalonitrile, on a heterogeneous catalyst, in the presence of liquid ammonia, in a reactor, whereby a part of the reactor product is continuously recycled to the reactor feed as a liquid recycle stream (recirculating loop). A flow of fused phthalonitrile is added as a liquid to the recycle stream around the hydrogenation reactor in a mixing device, whereby the phthalonitrile conversion in the reactor on a single pass is greater than 99 % and the recycle stream comprises more than 93 % by weight of liquid ammonia and diaminoxylene and contains no further solvent for phthalonitrile.
priorityDate 2003-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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