http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1642881-A4

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filingDate 2004-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2007-07-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-1642881-A4
titleOfInvention PROCESS FOR THE PRODUCTION OF 5-IODO-2-METHYLBENZOIC ACID
abstract A process for producing 5-iodo-2-methylbenzoic acid by iodizing 2-methylbenzoic acid, which comprises, as essential steps, a reaction step in which 2-methylbenzoic acid is iodized in the presence of a microporous compound, iodine, an oxidizing agent, and acetic anhydride and a purification step in which sublimation, distillation, crystallization, or a combination of two or more of these is conducted. By the process, 5-iodo-2-methylbenzoic acid, which is useful in functional chemicals such as medicines, can be easily obtained as a high-purity compound in a high yield. The production steps comprising reaction and separation/purification are simple from the standpoint of process operation and the purification load is small. Furthermore, the microporous compound, e.g., a zeolite catalyst, separated and recovered from the liquid resulting from the reaction can be repeatedly used after a simple treatment. Consequently, the catalyst has a long life and the target compound can be produced by the efficient process.
priorityDate 2003-07-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 27.