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filingDate 2003-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2004-12-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-1490663-A1
titleOfInvention A method and apparatus for automated analysis and characterization of chemical constituents of process solutions
abstract Method for direct automated analysis of a plurality analytes in a process solution (2). The method includes providing a sample of the process solution (4), admixing an enriched isotope spike for each of the plurality of analytes (20), creating ions from the analytes in the sample (26), introducing the ions to a mass spectrometer (28) to determine the identity and quantity of each analyte (34) and delivering the information to a microprocessor (36). The process may also include dilution of the sample (10) and/or addition of reagents (18) or standards (16) prior to initiation of analysis (6). The ions may be created through an atmospheric pressure ionization interface. Information is processed in the microprocessor (36) and serves to control addition of material to the process solution (2) and aspects of the process including sample extraction (4), sample handling (6), sample ionization (26) and the mass spectrometer (28). Apparatus for performing the process is also provided.
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