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filingDate 2003-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d826127ec747097cac526ad20bce8142
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publicationDate 2006-05-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-1468987-A4
titleOfInvention PROCESS FOR PRODUCING 2,4'-DIHYDROXYDIPHENYL SULFONE
abstract A process for producing 2,4'-dihydroxydiphenyl sulfone which comprises: subjecting a mixture which has been obtained by the dehydrating reaction of phenol with sulfuric acid or phenolsulfonic acid and contains 4,4'-dihydroxydiphenyl sulfone, 2,4'-dihydroxydiphenyl sulfone, phenolsulfonic acid, and phenol to crystallization to separate the 4,4'-dihydroxydiphenyl sulfone from the mixture and thereby obtain a mixture in which the content of 2,4'-dihydroxydiphenyl sulfone is not lower than that of 4,4'-dihydroxydiphenyl sulfone; regulating the mixture so as to have a solvent composition having a phenol/water ratio of from 10/90 to 90/10 by weight; crystallizing the 2,4'-dihydroxydiphenyl sulfone; and isolating the 2,4'-dihydroxydiphenyl sulfone by filtration. Also provided is a process for producing 2,4'-dihydroxydiphenyl sulfone in which the filtrate resulting from the filtration is utilized as a feed material for the subsequent dehydrating reaction.
priorityDate 2002-01-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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