http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-1163235-A2

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_2efbe95965e682e179dfd266c9980505
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D311-72
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-72
filingDate 2000-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f00bbdcade9e84a6e2ff79a3f8924fcb
publicationDate 2001-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-1163235-A2
titleOfInvention Methods for separating a tocopherol from a tocopherol-containing mixture and compositions thereof
abstract The invention relates to a method for separating tocopherol from a first tocopherol admixture by heating the first tocopherol admixture composed of at least one tocopherol, a fatty acid, and an esterifying compound to esterify the fatty acid to produce a second tocopherol admixture composed of the tocopherol, the esterified fatty acid, and the unesterified fatty acid; distilling the second tocopherol admixture with the esterified fatty acid to remove the unesterified fatty acid from the second tocopherol admixture to produce a third tocopherol admixture composed of the tocopherol, with substantially removed unesterified fatty acid; distilling the third tocopherol admixture for a sufficient time and temperature to substantially remove the tocopherol from the third tocopherol admixture to produce a fourth tocopherol admixture composed of the removed tocopherol and a non-tocol component; and extracting the tocopherol from the fourth tocopherol admixture with an extraction solvent composed of a polar, organic solvent that is miscible with water to produce a two phase system composed of a first phase containing the majority of the extraction solvent and the second phase, wherein the selectivity of the extraction solvent for tocopherol with respect to the non-tocol component is greater than unity, and removing the first phase from the second phase, with the proviso that the extraction solvent is not a neat alcohol. The invention further relates to compositions produced by the methods of the present invention.
priorityDate 1999-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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