http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0937712-A1

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filingDate 1998-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a835faa7428f80715d2ebb8ecc2f8ae9
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publicationDate 1999-08-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-0937712-A1
titleOfInvention Process for the preparation of E-caprolactam
abstract Process to prepare ε-caprolactam startingnfrom a starting mixture containing a 6-aminocaproatenester, in which in a first step (1) the 6-aminocaproatenester is converted into 6-aminocaproic acid and 6-aminocaproamidenby reaction with water in the presencenof ammonia at a temperature of between 50 and 250°C,nfollowed by a separate or simultaneous removal ofnalcohol(s), and in a subsequent step (2) the 6-aminocaproicnacid and 6-aminocaproamide are cyclizisednat an elevated temperature, wherein in step (1) the 6-aminocaproatenester is converted into 6-aminocaproicnacid and 6-aminocaproamide in the presence of an amountnhigher than 2 wt.% and less than or equal to 25 wt.% NH 3 n(relative to the total amount of organic compounds,nwater and ammonia present in step (1)).
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priorityDate 1998-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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