http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0801643-A1
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_0efa077d881a96aeb1e29b21ef1bbb58 |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-52 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D201-16 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D201-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D201-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B63-02 |
filingDate | 1995-12-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_44ed9ebf38da87d4be9eea8f2b980656 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_697885765f7cdb34a6ad2e2adb3e8c4e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f3391dbd8b9449d4f7186ea9abdb248a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_92360cf942b3ab9113cfae4e6a31b253 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c5e87ba40b9033e2515d4eec0aa4c438 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c1ef0e0baa9a529cc6bb1fa7d86ee3e2 |
publicationDate | 1997-10-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | EP-0801643-A1 |
titleOfInvention | Process for continuously cleaning raw caprolactam made from 6-amino capronitrile |
abstract | Cleaning raw caprolactam by hydration, subsequent treatment in an acid medium and final distillation in an alkaline medium, in which (a) 6-amino capronitrile is converted into raw caprolactam by reaction with water; (b) difficultly and easily boiling components are removed from the raw caprolactam from step (a); (c) the raw caprolactam from step (b) is treated with hydrogen at a temperature in the 50 to 150 DEG C range and a pressure in the 1.5 to 250 bar range in the presence of a hydration catalyst and, if desired, a solvent, to give a mixture A;(d1) mixture A is taken at a temperature in the 30 to 80 DEG C range and a pressure in the 1 to 5 bar range over an ion exchanger containing acid terminal groups to give a mixture B1 or (d2) mixture A is distilled in the presence of sulphuric acid, in which any solvent is removed before the addition of the sulphuric acid to give a mixture B2; and (e) mixture B1 or B2 is distilled in the presence of a base to yield pure caprolactam. |
priorityDate | 1995-01-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 86.