http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0475226-A2

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filingDate 1991-08-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_81a796381e0882c689a9474bda4523f7
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publicationDate 1992-03-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-0475226-A2
titleOfInvention Process for the preparation of 2-Mercapto-benzothiazole
abstract The invention relates to a process for the preparation of 2-mercaptobenzothiazole from aniline, sulfur and carbon disulfide under pressure and separation of the 2-mercaptobenzothiazole from the crude reaction product by cooling and recycling the by-products into the reactor together with aniline, sulfur and carbon disulfide, the reaction being carried out a residence time in the reactor of at least 1 hour at temperatures of 220-280 ° C and this terminated before reaching the reaction equilibrium and when cooling by mixing the crude reaction product with carbon disulphide above 100 ° C maintain the highest possible hydrogen sulfide pressure and the hydrogen sulfide only after crystallization of the 2-mercaptobenzothiazole is completely removed.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2005061471-A1
priorityDate 1990-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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