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filingDate 1989-04-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7a58876336311e0d4ca5712ba99009be
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publicationDate 1989-11-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-0341466-A1
titleOfInvention Process for the bromination of Nitroalcohols
abstract In a process for the production of geminal bromine nitro alcohols by bromination of alkali or alkaline earth metal salts of nitro alcohols, high concentrations should be used on an industrial scale. This was achieved by pumping a mixture of bromine and aqueous hydrogen bromide solution through a heat exchanger in a circuit and metering the aqueous solution of the alkali or alkaline earth metal salt of a nitro alcohol in front of the heat exchanger at a rate with cooling such that the maximum reaction temperature was 30 ° C. does not exceed.
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