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filingDate 1985-11-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_eb8f4fbd01012592856c7d7dc0aa9be1
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_74185e5161a93d96952dc90a3640ebec
publicationDate 1986-06-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-0184660-A1
titleOfInvention Monocyclic bis-oxyethylsulfonyl-benzenes and process for their preparation
abstract Compounds of the formula (1) <IMAGE> in which R is a hydrogen, chlorine or bromine atom or an alkylC1-C4 or alkoxyC1-C4 group and the two β-oxethylsulfonyl groups are in the o- or p-position to one another, and process for their preparation by converting a compound of formula (2) <IMAGE> in which the amino group is in the o- or p-position to the β-oxethylsulfonyl group after conversion into a diazonium halide with a mixture of alkali metal bisulfite and hydrohalic acid in the presence converted from copper or copper compounds at 0 ° C-50 ° C into the compound of formula (3) <IMAGE>, (2) the acid halide obtained with an alkali metal sulfite in an aqueous alkaline medium at pH 6-9 at 20-90 ° C converted into the alkali metal salt of sulfinic acid of the formula (4) <IMAGE>, (3) the sulfinate obtained in aqueous alkaline medium at pH 6-8 at 20-150 ° C. converted to bis-oxethylsulfonyl-benzene of the formula (5) < IMAGE>
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