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filingDate 1984-05-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1989-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 1989-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EP-0141481-B1
titleOfInvention Method of making polyimide foam precursor
abstract Methods of making low density modified polyimide! polyimide-amide foams and the resulting compositions. An N-substituted aliphatic imide is prepared by reacting a suitable aromatic dianhydride with a suitable oxime. A polyimide forming material is prepared by dissolving the N-substituted aliphatic imide in an esterifying solvent, then adding a suitable aromatic diamine. This material is dried to a powder. A suitable hydrated compound which is stable up to at least about 100°C. is mixed with the powder. A foam is then produced by heating the material to reaction temperature for a period sufficient to produce a stable foam. The material melts, then spontaneously expands into a foam which becomes self supporting and cures to a resilient flexible foam. The addition of the hydrated compound is found to result in an exceptionally low density foam. Depending upon heating conditions, a polyimide, polyimide- amide or mixture thereof may be produced, resulting in foams having selectively variable physical properties.
priorityDate 1983-11-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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